ХІМІЯ, ФІЗИКА ТА ТЕХНОЛОГІЯ ПОВЕРХНІ

ISSN 2518-1238 (Online), ISSN 2079-1704 (Print)

Приготування керамічних композитів на основі нанопорошків металу дозволяють значно змінити теплові характеристики керамічної матриці, що важливо для створення технології теплопровідної кераміки.

В роботі встановлений максимально ефективний спосіб отримання нанопорошку нікелю на потенціостаті «П-5848» електролізом cульфату нікелю (NiSO₄) з додаванням борної кислоти (H₃BO₃), тіосечовини ((NH₄)₂CS) та хлориду нікелю (II) (NiCl₂). Синтез нанопорошку Ni проводився при густині струму від 1.0 до 3.3 А/дм² та при температурі 45–65 °С, де анодом була обрана платинова (Pt) пластина, а катод був спеціально виготовлений з особливо чистого алюмінію (Al). Результати дослідження показали синтез нанопорошку Ni при розмірі 55 нм у вигляді тонких лусок. В роботі також розглянуті електрохімічні реакції на катоді та на аноді.

Також в роботі проведено декілька вдалих експериментів, що дозволили встановити економічно вигідну технологію синтезу нанопорошку міді методом електролізу при 13.3 ампер-годин струму на 1 дм² площини аноду та при відносно низькій температурі розчину сульфату міді (CuSO₄). Мідний нанопорошок видаляється на дно ванни з аноду при ударному струшуванні. Не менш вдалий був проведений експеримент, де був катод у вигляді декількох мідних пластин на відстані 0.8 см одне від одного з напругою між ними в 0.775 В, та густиною струму 15.3 А/дм² при температурі 54 °С в електроліті з 45 % H₂SO₄, 8 % Na₂SO₄ і 4 % CuSO₄.

В роботі наведені таблиці з вихідними та кінцевими даними всіх експериментів з синтезу нанопорошків методом електролізу.

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